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Photocatalytic ATRP Depolymerization: Temporal Control at Low ppm of Catalyst Concentration

https://doi.org/10.1021/jacs.3c05632

Parkatzidis, Kostas ; Truong, Nghia P. ; Matyjaszewski, Krzysztof ; Anastasaki, Athina ( September 2023 , Journal of the American Chemical Society)
A comparison of RAFT and ATRP methods for controlled radical polymerization

https://doi.org/10.1038/s41570-021-00328-8

Truong, Nghia P. ; Jones, Glen R. ; Bradford, Kate G. ; Konkolewicz, Dominik ; Anastasaki, Athina ( December 2021 , Nature Reviews Chemistry)

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Practical Chain-End Reduction of Polymers Obtained with ATRP

https://doi.org/10.1002/macp.201700107

Gutekunst, Will R. ; Anastasaki, Athina ; Lunn, David J. ; Truong, Nghia P. ; Whitfield, Richard ; Jones, Glen R. ; Treat, Nicolas J. ; Abdilla, Allison ; Barton, Bryan E. ; Clark, Paul G. ; et al ( September 2017 , Macromolecular Chemistry and Physics)
One‐Pot Synthesis of ABCDE Multiblock Copolymers with Hydrophobic, Hydrophilic, and Semi‐Fluorinated Segments

https://doi.org/10.1002/anie.201707646

Anastasaki, Athina ; Oschmann, Bernd ; Willenbacher, Johannes ; Melker, Anna ; Van Son, Martin H. C. ; Truong, Nghia P. ; Schulze, Morgan W. ; Discekici, Emre H. ; McGrath, Alaina J. ; Davis, Thomas P. ; et al ( October 2017 , Angewandte Chemie International Edition)

Abstract
The scope and accessibility of sequence‐controlled multiblock copolymers is demonstrated by direct “in situ” polymerization of hydrophobic, hydrophilic and fluorinated monomers. Key to the success of this strategy is the ability to synthesize ABCDE, EDCBA and EDCBABCDE sequences with high monomer conversions (>98 %) through iterative monomer additions, yielding excellent block purity and low overall molar mass dispersities (Ð<1.16). Small‐angle X‐ray scattering showed that certain sequences can form well‐ordered mesostructures. This synthetic approach constitutes a simple and versatile platform for expanding the availability of tailored polymeric materials from readily available monomers.

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One‐Pot Synthesis of ABCDE Multiblock Copolymers with Hydrophobic, Hydrophilic, and Semi‐Fluorinated Segments

https://doi.org/10.1002/ange.201707646

Anastasaki, Athina ; Oschmann, Bernd ; Willenbacher, Johannes ; Melker, Anna ; Van Son, Martin H. C. ; Truong, Nghia P. ; Schulze, Morgan W. ; Discekici, Emre H. ; McGrath, Alaina J. ; Davis, Thomas P. ; et al ( October 2017 , Angewandte Chemie)

Abstract
The scope and accessibility of sequence‐controlled multiblock copolymers is demonstrated by direct “in situ” polymerization of hydrophobic, hydrophilic and fluorinated monomers. Key to the success of this strategy is the ability to synthesize ABCDE, EDCBA and EDCBABCDE sequences with high monomer conversions (>98 %) through iterative monomer additions, yielding excellent block purity and low overall molar mass dispersities (Ð<1.16). Small‐angle X‐ray scattering showed that certain sequences can form well‐ordered mesostructures. This synthetic approach constitutes a simple and versatile platform for expanding the availability of tailored polymeric materials from readily available monomers.

more » « less